Qualitative Analysis II Introduction: In this prove procedures were devised that enabled us to furcate, properly mention mixtures of sextet different cations. by and by each cation is identified the procedures that were devised were used to identify which cations were present in an unknown solution. Qualitative analysis deals with the insularity and identification of sextuplet cations: Ag+, Al3+, Ba2+, Ca2+, Fe3+, and Pb2+. Solubility equilibria, amphoterism, and complex-ion equilibria play important roles in the breakup and identification of the unknown solution. Procedure: Test to Establish familiar Classes (first week) - First testify thermionic tubes were obtained, and cleaned. Next the solutions of silver nitrate, aluminum nitrate, barium nitrate calcium nitrate, iron (III) nitrate, and lead (II) nitrate were each put in into test tubes, and labeled. Next, the HCl was added and mixed thoroughly, and observations were recorded. Next sunrise(prenominal) c ations were put into new test tubes, and the same test was ran with buffered ammonia, and so with ammonium ion carbonate. Then all of the settles from each test were centrifuged, and decanted. The precipitates were all serve to remove all of the ammonium carbonate. The precipitates were treated with HCl, and observations were recorded. Dividing the Cations into oecumenic Classes- utilize the results obtained from the preceding tests schemes for separating the six cations into three general classes by end the flow charts.
Examining the Hydrochloric Acid Class- First twenty drops of the 0.1M solutions conta ining the nitrates of the cations were put ! into separate test tubes, and labeled. Then hydrochloric acid was added, and each tube was centrifuged. go down was decanted and then washed. The precipitation was then set in a boiling bath, and stirred routinely. Potassium chromate was added to the test tube that the precipitate dissolved. The water was then decanted from the precipitate that didnt dissolve, and ammonia... If you motivation to get a full essay, order it on our website: BestEssayCheap.com
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